[et_pb_section fb_built=”1″ _builder_version=”4.9.4″ _module_preset=”default” background_color=”#e4e4e4″ positioning=”none” custom_padding=”12px||6px|||” sticky_position=”top” border_width_bottom=”2px” border_color_bottom=”#f4f4f4″ box_shadow_style=”preset3″ global_colors_info=”{}”][et_pb_row column_structure=”1_3,1_3,1_3″ use_custom_gutter=”on” gutter_width=”1″ make_equal=”on” _builder_version=”4.9.4″ _module_preset=”default” max_width=”80%” custom_margin=”|auto|8px|auto||” custom_padding=”1px||0px|||” global_colors_info=”{}”][et_pb_column type=”1_3″ _builder_version=”4.9.4″ _module_preset=”default” border_color_all=”#FFFFFF” global_colors_info=”{}”][\/et_pb_column][et_pb_column type=”1_3″ _builder_version=”4.9.4″ _module_preset=”default” background_enable_color=”off” link_option_url=”http:\/\/sai.unizar.es\/solPrestSAI\/” link_option_url_new_window=”on” border_radii=”on|15px|15px|15px|15px” border_width_all=”2px” border_color_all=”#bababa” global_colors_info=”{}” background__hover_enabled=”on|hover” background_color__hover=”#FFFFFF” background_enable_color__hover=”on”][et_pb_text _builder_version=”4.14.2″ _module_preset=”default” text_font=”|||on|||||” text_text_color=”#333333″ text_font_size=”14px” link_text_color=”#333333″ background_enable_color=”off” custom_margin=”||4px|||” custom_padding=”|5px||5px|true|true” hover_enabled=”0″ border_color_all=”RGBA(0,0,0,0)” border_color_right=”#FFFFFF” border_color_left=”#FFFFFF” global_colors_info=”{}” link_text_color__hover_enabled=”on|hover” link_text_color__hover=”#4370b4″ sticky_enabled=”0″]<\/p>\n
Access on demand<\/strong><\/a><\/p>\n [\/et_pb_text][\/et_pb_column][et_pb_column type=”1_3″ _builder_version=”4.9.4″ _module_preset=”default” border_color_all=”#FFFFFF” global_colors_info=”{}”][\/et_pb_column][\/et_pb_row][\/et_pb_section][et_pb_section fb_built=”1″ _builder_version=”4.9.4″ _module_preset=”default” custom_padding=”25px||25px|||” global_colors_info=”{}”][et_pb_row column_structure=”1_2,1_2″ _builder_version=”4.9.4″ _module_preset=”default” max_width=”75%” custom_padding=”||6px|||” global_colors_info=”{}”][et_pb_column type=”1_2″ _builder_version=”4.9.4″ _module_preset=”default” global_colors_info=”{}”][et_pb_text _builder_version=”4.9.4″ _module_preset=”default” text_font_size=”16px” text_line_height=”2em” ul_line_height=”2em” header_2_font=”|700|||||||” header_2_font_size=”23px” custom_margin=”||-8px|||” custom_padding=”||40px|||” global_colors_info=”{}”]<\/p>\n The X-ray Diffractometer PANalytical Empyrean is a multipurpose diffractometer that offers a wide range of diffraction geometries: reflection, transmission, capillary, Debye-Scherrer, Graze Incident X-ray Diffraction (GIXRD), Small and Wide Angle Scatering (SAXS & WAXS)\u2026 Combining different available sets of optical components and sample stages it has the ability to analyze a wide range of samples such a powders, solid objects, thin films, dispersions\u2026 Thanks to the PreFIX concept it is possible to exchange between the operation modes \/ configurations\u00a0 in few minutes without the need to realign the system. The diffractometer is equipped with <\/span>PIXcel1D detector. A dedicated strip detector for 0D and 1D applications which allows to\u00a0 measure up to 255 times faster than with a traditional point detector, without compromising data quality<\/span>.\u00a0<\/span><\/p>\n The laboratory is complemented with the powerful HighScore analysis Software. From phase identification to Rietveld analysis. Using a Full pattern approach <\/span>HighScore is the ideal software for phase identification, semi-quantitative phase analysis, pattern treatment, profile fitting and more<\/span>.<\/span><\/p>\n [\/et_pb_text][\/et_pb_column][et_pb_column type=”1_2″ _builder_version=”4.9.4″ _module_preset=”default” global_colors_info=”{}”][et_pb_image src=”https:\/\/lma.unizar.es\/wp-content\/uploads\/2022\/01\/XRD_PAN_1200x800-scaled-e1642419074952.jpg” title_text=”XRD_PAN_1200x800″ align=”center” _builder_version=”4.14.2″ _module_preset=”default” custom_margin=”||11px|||” border_radii=”on|15px|15px|15px|15px” border_width_all=”1px” global_colors_info=”{}”][\/et_pb_image][\/et_pb_column][\/et_pb_row][et_pb_row _builder_version=”4.9.4″ _module_preset=”default” max_width=”75%” custom_margin=”4px|auto||auto||” custom_padding=”5px|||||” global_colors_info=”{}”][et_pb_column type=”4_4″ _builder_version=”4.9.4″ _module_preset=”default” global_colors_info=”{}”][et_pb_text _builder_version=”4.9.4″ _module_preset=”default” text_font_size=”16px” text_line_height=”2em” ul_line_height=”2em” header_2_font=”|700|||||||” header_2_font_size=”23px” global_colors_info=”{}”]<\/p>\n [\/et_pb_text][\/et_pb_column][\/et_pb_row][\/et_pb_section][et_pb_section fb_built=”1″ _builder_version=”4.9.4″ _module_preset=”default” custom_padding=”39px||40px|||” global_colors_info=”{}”][et_pb_row use_custom_gutter=”on” make_equal=”on” _builder_version=”4.9.4″ _module_preset=”default” max_width=”75%” global_colors_info=”{}”][et_pb_column type=”4_4″ _builder_version=”4.9.4″ _module_preset=”default” global_colors_info=”{}”][et_pb_tabs active_tab_background_color=”#2ea3f2″ inactive_tab_background_color=”#4370b4″ active_tab_text_color=”#FFFFFF” _builder_version=”4.9.4″ _module_preset=”default” tab_text_color=”#FFFFFF” tab_font=”|700||on|||||” tab_font_size=”15px” tab_line_height=”3em” custom_margin=”||||false|false” custom_padding=”||||false|false” border_radii=”on|15px|15px|15px|15px” global_colors_info=”{}”][et_pb_tab title=”What kind of information can be obtained?” _builder_version=”4.9.4″ _module_preset=”default” global_colors_info=”{}”]<\/p>\n Whether you are interested in improved process control, or doing research and development, understanding your materials starts very often with understanding the powder diffraction pattern. <\/span>Traditionally X-ray powder diffraction is most widely used for the characterization of unknown crystalline materials. Determination of unknown solids is fundamental material science, engineering, geology, and biology. Nowadays capabilities of XRD include new applications and XRD is useful for a wider range of materials including not only inorganic materials, but also polymers, nanomaterials, dispersions, composites, soft materials, coatings\u2026<\/span><\/p>\n Dimensional and structural characterization of nanomaterials:<\/strong><\/span><\/p>\n GIXRD and reflectivity:<\/strong> Characterization of Thin films and multilayers. Stress, thickness, roughness and density. Depth profiles.<\/p>\n Non-ambient XRD:<\/strong> In-situ studies of temperature-induced phase transformations and changes of structural properties (strain, grain size, phase composition, order-disorder transformations, thermal expansion\u2026).<\/p>\n [\/et_pb_tab][et_pb_tab title=”Sample requirements” _builder_version=”4.9.4″ _module_preset=”default” global_colors_info=”{}”]<\/p>\n The PANalytical Empyrean diffractometer is capable to manage <\/span>with a wide range of samples: Inorganics, polymers, nanostructured materials, soft materials\u2026 They can be in the form of bulk materials, powders, foils, thin films, gels,\u00a0 liquids, dispersions\u2026<\/span><\/p>\n When working with large and heavy samples the 3-axes Empyrean cradle enables analysis of components weighing up to 2 kg. Parallel-beam geometry can be used for the phase identification of rough and irregularly shaped objects.<\/span><\/p>\n Different sample holders are available for Transmission and reflection X-ray depending on the available amount of sample and geometry and zero background holders to be used when only small amount of powdered sample is available.<\/span><\/p>\n [\/et_pb_tab][et_pb_tab title=”Technical specifications and capabilities” _builder_version=”4.9.4″ _module_preset=”default” global_colors_info=”{}”]<\/p>\n X-RAY Generator \/ Tube<\/b><\/p>\n Goniometer<\/b><\/p>\n Incident Beam optics\u00a0\u00a0<\/b><\/p>\n Diffracted Beam optics<\/b><\/p>\n Detector: <\/b>PIXcel<\/i><\/b>1D<\/i><\/b> Medipix3<\/i><\/b>\u00a0<\/span><\/p>\n Reflection Transmission Spinner\u00a0<\/b><\/p>\n Back loading on \u00d816 and \u00d827 mm\u00a0<\/span><\/p>\n Zero Background Holders\u00a0<\/span><\/p>\n Irregular samples: max [mm] \u00d844, 6.5 thick\u00a0<\/span><\/p>\n Transmission between foils\u00a0<\/span><\/p>\n HTK 1200N with capillary extension\u00a0\u00a0<\/b><\/p>\n . \u00d816 mm (0.4 and 0.8 deep) for reflection\u00a0<\/span><\/p>\n . 1 mm quartz capillaries for transmission<\/span><\/p>\n Three-Axes (Z, Phi, Chi) cradle 10\u00a0<\/b><\/p>\n ScatterX<\/b>78<\/b><\/p>\n HighScore 4.1 11\u00a0<\/b><\/p>\n [\/et_pb_tab][\/et_pb_tabs][\/et_pb_column][\/et_pb_row][\/et_pb_section][et_pb_section fb_built=”1″ _builder_version=”4.9.4″ _module_preset=”default” min_height=”179px” custom_margin=”9px||-9px|||” custom_padding=”0px||4px|||” global_colors_info=”{}”][et_pb_row use_custom_gutter=”on” gutter_width=”4″ _builder_version=”4.9.4″ _module_preset=”default” max_width=”75%” custom_margin=”0px|auto||auto||” custom_padding=”55px||||false|false” global_colors_info=”{}”][et_pb_column type=”4_4″ _builder_version=”4.9.4″ _module_preset=”default” global_colors_info=”{}”][et_pb_gallery gallery_ids=”2911,2910,2909″ posts_number=”3″ show_title_and_caption=”off” show_pagination=”off” module_class=”ilogos” _builder_version=”4.9.4″ _module_preset=”default” global_colors_info=”{}”][\/et_pb_gallery][\/et_pb_column][\/et_pb_row][\/et_pb_section][et_pb_section fb_built=”1″ _builder_version=”4.9.4″ _module_preset=”default” use_background_color_gradient=”on” background_color_gradient_start=”#000000″ background_color_gradient_end=”rgba(0,0,0,0.48)” background_color_gradient_overlays_image=”on” background_image=”https:\/\/lma.unizar.es\/wp-content\/uploads\/2021\/10\/render-lma-1.jpg” custom_margin=”9px|||||” custom_padding=”||42px|||” saved_tabs=”all” global_colors_info=”{}”][et_pb_row column_structure=”1_3,1_3,1_3″ use_custom_gutter=”on” gutter_width=”2″ _builder_version=”4.9.4″ _module_preset=”default” max_width=”75%” global_colors_info=”{}”][et_pb_column type=”1_3″ _builder_version=”4.9.4″ _module_preset=”default” global_colors_info=”{}”][et_pb_text _builder_version=”4.9.4″ _module_preset=”default” text_text_color=”#FFFFFF” text_line_height=”2em” global_colors_info=”{}”]<\/p>\n Laboratorio de Microscop\u00edas Avanzadas\n<\/p>\n We are a unique initiative at national and international levels. We provide the scientific and industrial community with the most advanced infrastructures in Nanofabrication, Local Probe and Electron Microscopies for the observation, characterization, nanopatterning and handling of materials at atomic and molecular scale.[\/et_pb_text][\/et_pb_column][et_pb_column type=”1_3″ _builder_version=”4.9.4″ _module_preset=”default” global_colors_info=”{}”][et_pb_text _builder_version=”4.9.4″ _module_preset=”default” text_text_color=”#FFFFFF” link_text_color=”#FFFFFF” global_colors_info=”{}”]<\/p>\n Contact information<\/p>\n Campus R\u00edo Ebro, Edificio Edificio I+D+i<\/p>\n Tel.:(+34) 976 762 980 <\/strong><\/a><\/span>AVAILABLE SAMPLE STAGES<\/h2>\n
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